Analytic laboratory services Analytic laboratory services Contents 1. 2. 3. 4. 4.1. 4.2. 4.3. 4.4. Competence Main activities Services offered Parameter Parameter of Water and waste water analysis Organic parameter Microbiological tests Further analysis parameters Status: July 2012 1 Analytic laboratory services The department analytic laboratory services of InfraLeuna is: a testing laboratory accredited by the DAkkS (Deutsche Akkreditierungsstelle - German Accreditation Body) according to DIN EN ISO/IEC 17025. The accreditation is for, as mentioned in the certificate of accreditation, the listed procedures; a listed analytical investigation body for drinking water pursuant to § 15 par. 4 sentence 1 of the drinking water ordinance 2001 for physical, physico-chemical, chemical and microbiological analysis drinking water; certified according to DIN EN ISO 9001, DIN EN 14001 and SCC-checklist. Manfred Witte Head of Water Supply/disposal/Analytic laboratory services Phone: +49 (0)3461-43 4283 Fax: +49 (0)3461-43 8532 Email: m.witte@infraleuna.de Dr. Antje Mroczek Head of Analytic laboratory services Phone: +49 (0)3461-43 6467 Fax: +49 (0)3461-43 3165 Email: analytik @infraleuna.de Status: July 2012 2 Analytic laboratory services 1. Competence We are your competent contact person concerning analytical problems of the water, waste water, product, fouling and waste analysis. Due to our immediate vicinity to your plants and many years of experience in analytical monitoring of industrial plants for water treatment, waste water treatment, power generation and of closed cooling systems you can benefit of many advantages. Our range of services comprises nearly all standard methods of the water and waste water, the inorganic and organic trace analysis and the microbiology. Appropriate analysis methods can be chosen targeted for the solution of your problems. The results are transferred to you in requested form after short processing time. Our modern laboratory and information management system offers the possibility to prepare the analysis results in a test report or in table form and transmit them via email or fax. Furthermore the undertaking of complex laboratory analytical monitoring tasks for the process management of your plants ranging from the sampling to the daily result transmission is part of our range of services. Contact persons: Dr. Antje Mroczek Head of Analytic laboratory services Inorganic-instrumental analysis Tel.: +49 (0)3461-43 6467 Dr. Peter Thomas Zenner Organic-instrumental analysis Tel.: +49 (0)3461-43 3790 Heike Lange Wastewater and water analysis Tel.: +49 (0) 3461-43 5330 Sigrid Bamps Water analysis and microbiology Tel.: +49 (0)3461-43 8032 Silvia Weineck Laboratory organization-sample management, sampling, microbiology Tel.: +49 (0)3461-43 3151 Sample management Tel.: +49 (0)3461-43 3176 Fax: +49 (0)3461-43 3165 Status: July 2012 3 Analytic laboratory services 2. Main activities Analysis accompanying processes and analytical monitoring of quality parameter: Industrial water treatment: - fresh water and industrial water treatment, - condensate and feed water treatment, - e.g. analytical monitoring of decarbonization, coagulation, reverse osmosis, desalination, ion exchanger; Power generation plants and steam generators: - monitoring of water-steam circulations according to statutory regulations (VGB and VdTÜV), - ultrapure water analysis, - flue gas desulphurization, REA-plaster (according to VGB-M 701); Cooling circuits: - cooling water treatment, cooling water conditioning, - microbiological testing in cooling circuits; Waste water treatment: - waste water declaration analysis, - control of waste water discharges according to statutory regulations, - supervision of biological waste water treatment plants; Drinking water analysis, hot water systems (chemically, physical-chemically, microbiologically): - drinking water treatment, distribution networks, - installation of in-house water systems, - water pipe releases; Ground water analysis: - ground water purification plant, - ground water gauge networks, - landfill leachates; Check of measuring devices by means of on-site laboratory testing and control testing with portable testing facilities; Development of customer-specific solutions and standards for measuring devices; Waste and residue analysis: - declaration analysis relating to the landfill (LAGA-regulations, TA Abfall), - declaration analysis for the reassembly at the chemical site Leuna; Composition of foulings in industrial plants. 3. Services offered On over 1,200 sqm laboratory area with over 20 qualified, permanent employees in immediate customer vicinity we give the warranty for a reliable, competent and long-standing secured cooperation on a technically advanced level. Due to our modern equipment technology we can offer you a comprehensive parameter spectrum of various sample matrices. Status: July 2012 4 Analytic laboratory services Sampling: - drinking water - waste water - ground water - waste, building rubble; Element determination: - elemental analysis (C, S) , - determination of elements with the help of atomic spectroscopy (e.g. Ca, Mg, Na, K, Ba, Sr, Pb, Cd, Cr, Cu, Ni, Zn, As, Se, Sb, Ti, V, Mn, Mo, Pt, Fe, Co, Pd, Ag, Al, Tl, Sn, P, Hg) ranging from the ultra trace range to the main components, - semiquantitative overview analysis, - different sample pretreatment and pulping technologies; Samples matrices: - water (drinking water, ground water, cooling water, deonized water, permeate, feed water, ultrapure water, steam condensate, etc.), - waste water - products (e.g. acids, salts, hydrogen peroxide, methanol, gypsum, calcium carbonate, polymers), - waste, building rubble, - foulings - sludge, - fuels, oil and refinery products. 4. Parameter 4.1. Parameter of water and waste water analysis pH-value electrical conductivity temperature redox potential oxygen coloration clouding hardness (total- carbonate- and noncarbonate hardness) acid and base capacity permanganate index particle size distribution phenol index carbon compounds (TOC, DOC, TIC) calcite saturation according to DEV C10-R3 ammonium chloride nitrate sulfate nitrite bromate sulfide sulfite fluoride anionic surfactants ((MBAS) cyanide easily purgeable silicic acid iron (total, dissolved, Fe II) hydrazine Status: July 2012 5 Analytic laboratory services AOX (absorbable organic halogen) nitrogen compounds (TNB) biochemical oxygen demand (5 days) chemical oxygen demand nitrification inhibition test depletion test biodegradability (Zahn-Wellens-test) total phosphor orthophosphate free chlorine lipophilic substances filtratable solids filtrate dry residue settleable solids suspended solids 4.2. Organic parameter BTEXC (benzene, toluene, ethyl benzene, xylene, cumene) LHKW ( lightly volatile halogenated hydrocarbons) MTBE Methanol Carbonic acids (C1 – C6) PAK (polycyclic aromatic hydrocarbon) GC-MS-overview analysis (qualitative screening) Hydrocarbon index IR-spectra measurement 4.3. Microbiological tests Pipe release Monitoring of cooling circuits (Colony number, legionella) Colony number Escherichia coli, coli form germs Enterococci Pseudomonas aeruginosa Legionella Yeasts, fungus Status: July 2012 6 Analytic laboratory services 4.4. Further analysis parameters Dry residue Ignition loss, ignition residue Sludge volume index Water-soluble part Determination out of the eluate (DIN 38414 S4) Determination out of the aqua regia extract (DIN 38414 S7) Microscopical analysis of activated sludge Status: July 2012 7